공학 열분석(Thermal analysis)

공학 열분석(Thermal analysis)

[공학] 열분석(Thermal analysis).pptx

목차 1.Thermal analysis??? 2.TGA(ThermoGravimetry analysis) 3.DSC (Differential Scanning Calorimeter) 4.DTA(Differential Thermal Analysis) 5.Application 6.Thermal Analysis Examples 7.Decomposition of CaC2O4 H2O 9.Precipitated Zr5O8(SO4)2 15 H2O 10.Analysis of Filtrate from Precipitation 11.Polyethylene 12.Nylon compositional analysis 13.Thermal Decomposition ofBH3NH3 14.Thermograms for commonPolymeric materials 15.Flame retardancy 16.Adsorption and Desorption of CO2 On Active coal 17.Organic CompoundBenzoic Acid 18.Inorganic CompoundCalcium Oxalate 19.Oxidation or ThermalDecomposition Reaction 20.Application of ThermalAnalyses to Li-ion Batteries 21.Li-ion Batteries 22.Cathode 23.LiCoO2(Lithium Cobalt Oxide) 24.LiFePO4 Olivine(Lithium Iron Phosphate) 25.Layer Coating 26.MCMB(Mesocarbon Microbead) 27.Electolytes 28.PP Separator(polypropylene) 본문 instrument composition -Electric furnace Temperature range: 25°C~1500°C Heat speed : Maximum 200°C/min *Separate Electric furnace and other system like Electronic scale -Because Electric furnace temperature is very high so we need to protect other system. instrument composition -Electric furnace Temperature range: 25°C~1500°C Heat speed : Maximum 200°C/min *Nitrogen or Argon in Electric furnace -Because the inhibition of oxidization of sample 참고문헌 Ellis, B. L.; Lee, K.T.; Nazar, L.F. Chem. Mater. 2010, 22, 691 714 Gu, Y.; Chen, D.*; Jiao, X. J. Phys. Chem. B 2005, 109, 17901-17906 Quinlan, F.T.; Vidu, R.; Predoana, L.; Zaharescu, M.; Gartrner, M.; Groza, J.; Stroeve, P.* Ind. Eng. Chem. Res. 2004, 43, 2468-2477 Zhang, Z.*; Fouchard, D.; Rea, J.R. Journal of Power Sources 1998, 70, 16-20 Dahn, J.R.; Fuller, E.W.; Obrovac, M.; Sacken, U. von. Solid State Ionics 1994, 69, 265-270 Lyczko, N.; Nzihou, A.; Sharrock, P.; Germeau, A.; Toussaint, C. Ind. Eng. Chem. Res. 2011, Just Accepted Manuscript Myung, S.T.*; Lee, K.S.; Yoon, C.S.; Sun, Y.K.*; Amine, K.; Yashiro, H. J. Phys. Chem. C 2010, 114, 4710 4718 MacNeila, D.D.*; Dahn, J.R. Journal of The Electrochemical Society 2003, 150, A21-A28 Li, B.; Guo, R.; Li, K.; Lu, C.; Ling, L. Fuel Chemistry Division Preprints 2002, 47, 187-188 김영준. "리튬이차전지 핵심 부품소재 특성 평가". 2009. 40. 2010 이차전지 산업 전망 및 핵심 기술 이슈 세미나. 차세대전지연구센터, KETI. Skoog, D.A.; Holler, F.J.; Crouch, S.R. Principles of Instrumental Analysis (6th Edition) . 2007. 894-904. Stanford University, University of Kentucky, and Michigan State University. Thomson Brook/Cole. West, A.W. Basic Solid Chemistry (2nd Edition) . 1999. 203-210. Department of Engineering Materials, Sheffield University. John Wiley & Sons, Ltd. 송연호, 양원강, 태범석, 이경호, 박영조. 분석화학 . 2007. 343-347. AUDAX publishers. 박면용, 정우식, 양원강, 김동엽, 서무룡, 권수한, 이경호. 기기분석 . 2006. 536-552. 기기분석교재연구회. 녹문당. 키워드 Thermal, 열분석, analysis, 공학